Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra

CORC > 武汉物理与数学研究所 > 中国科学院武汉物理与数学研究所 > 2011年以前论文发表（包括2011年）

	Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra
	Li, N ; Yao, KM ; Lou, KY ; Shen, LF ; Yuan, HZ
刊名	SCIENCE IN CHINA SERIES B-CHEMISTRY
	1999-12-01
卷号	42 期号:6 页码:599-604
关键词	Ln(III) complexes with Schiff base high resolution solid state C-13 NMR liquid state 2D-H-1-C-13 COSYNMR CPMAS TOSS
英文摘要	La(III),Y(III) complexes with diglycol aldehyde bis-arginine (H(2)DAAR) and tetraglycol aldehyde bis-lysine (H(2)TALY) Schiff bases were synthesized. They were characterized and formulated as La( H(2)DAAR)(NO3)(3). 6H(2)O and Y(H(2)TALY) (NO3)(3) . 5H(2)O separately by elemental analyses. The obtained complexes were investigated in detail by high resolution solid state (HRSS) C-13 NMR using cross polarization, magic angle spinning (CPMAS), and total suppression of sidebands (TOSS) techniques. The results are supported by the liquid state 2D-(1) H-C-13 COSY NMR spectra. Some new information about the splitting peaks of C-13 for -CH=N- soup and alkene carbon bands, etc. in HRSS C-13 NMR spectra are given.
WOS标题词	Science & Technology ; Physical Sciences
类目[WOS]	Chemistry, Multidisciplinary
研究领域[WOS]	Chemistry
关键词[WOS]	GADOLINIUM COMPLEXES ; EPR-SPECTRA
收录类别	SCI
语种	英语
WOS记录号	WOS:000084653800006
公开日期	2015-12-01
内容类型	期刊论文
源URL	[http://ir.wipm.ac.cn/handle/112942/8362]
专题	武汉物理与数学研究所_2011年以前论文发表（包括2011年）
作者单位	1.Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China 2.Chinese Acad Sci, Wuhan Inst Phys & Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China
推荐引用方式 GB/T 7714	Li, N,Yao, KM,Lou, KY,et al. Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra[J]. SCIENCE IN CHINA SERIES B-CHEMISTRY,1999,42(6):599-604.
APA	Li, N,Yao, KM,Lou, KY,Shen, LF,&Yuan, HZ.(1999).Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra.SCIENCE IN CHINA SERIES B-CHEMISTRY,42(6),599-604.
MLA	Li, N,et al."Synthesis of La(III), Y(III) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state C-13 NMR spectra".SCIENCE IN CHINA SERIES B-CHEMISTRY 42.6(1999):599-604.