Chromatographic Evaluation of Octadecyl-Bonded SiO2/SiO2-Based Stationary Phase for Reversed-Phase High Performance Liquid Chromatography

CORC > 兰州化学物理研究所 > 中国科学院兰州化学物理研究所 > 中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室

	Chromatographic Evaluation of Octadecyl-Bonded SiO2/SiO2-Based Stationary Phase for Reversed-Phase High Performance Liquid Chromatography
	Zhang X(张霞)1,2,3 ; Zhang ZX(张志欣)1,2; Wang LT(王利涛)1,2 ; Liu Q(刘芹)1,2; Zhang XL(张晓莉)1,2,3; Dong SQ(董树清)1,2 ; Zhao L(赵亮)1,2 ; Zhao L(赵亮)
刊名	Journal of Inorganic and Organometallic Polymers and Materials
	2013
卷号	23 期号:6 页码:1445-1450
关键词	Core–shell microspheres HPLC Octadecyl-bonded SiO2/SiO2 stationary phase Octadecyl-bonded SiO2 stationary phase Reversed-phase
ISSN号	1574-1443
通讯作者	赵亮
英文摘要	A new type of octadecyl-bonded SiO₂/SiO₂ (ODSS) core-shell monodisperse silica spheres was prepared as a high performance liquid chromatography stationary phase. The chromatographic performance was evaluated and compared with totally porous octadecyl-bonded SiO₂. Various methods were used for characterization of the two column packings for reversed-phase chromatography in terms of permeability, hydrophobic selectivity, sensitivity, stability and hydrophobicity. The results showed that the ODSS-based stationary phase has enhanced permeability, good hydrophobic selectivity, high chemical stability and sensitivity. Acidic, basic and neutral aromatic compounds were separated on the two types of stationary phases. The ODSS-based stationary phase has good selectivity and gives symmetrical narrow peaks under reversed-phase conditions.
学科主题	分析化学与药物化学
收录类别	SCI
资助信息	the National Nature Science Foundation of China (Grant: 20675085);Science and Technology Support Xinjiang Project (2010);the Science and Technology Special Project of Lanzhou (No. 2010-1-156)
语种	英语
WOS记录号	WOS:000325430500031
公开日期	2013-12-10
内容类型	期刊论文
源URL	[http://210.77.64.217/handle/362003/4581]
专题	兰州化学物理研究所_中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室
通讯作者	Zhao L(赵亮)
作者单位	1.Chinese Acad Sci, Key Lab Chem Northwestern Plant Resources, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China 2.Chinese Acad Sci, Key Lab Nat Med Gansu Prov, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China 3.Univ Chinese Acad Sci, Beijing 100039, Peoples R China
推荐引用方式 GB/T 7714	Zhang X,Zhang ZX,Wang LT,et al. Chromatographic Evaluation of Octadecyl-Bonded SiO2/SiO2-Based Stationary Phase for Reversed-Phase High Performance Liquid Chromatography[J]. Journal of Inorganic and Organometallic Polymers and Materials,2013,23(6):1445-1450.
APA	Zhang X.,Zhang ZX.,Wang LT.,Liu Q.,Zhang XL.,...&赵亮.(2013).Chromatographic Evaluation of Octadecyl-Bonded SiO2/SiO2-Based Stationary Phase for Reversed-Phase High Performance Liquid Chromatography.Journal of Inorganic and Organometallic Polymers and Materials,23(6),1445-1450.
MLA	Zhang X,et al."Chromatographic Evaluation of Octadecyl-Bonded SiO2/SiO2-Based Stationary Phase for Reversed-Phase High Performance Liquid Chromatography".Journal of Inorganic and Organometallic Polymers and Materials 23.6(2013):1445-1450.