Synthesis and characterization of zeolite mazzite analogue in Na2O-Al2O3-SiO2-Piperazine-H2O
Xu, H.; Dong, P.; Liu, L.; Wang, J.-G.; Deng, F.; Dong, J.-X.
刊名JOURNAL OF POROUS MATERIALS
2007-03-01
卷号14期号:1页码:97-101
关键词zeolite mazzite analogue piperazine synthesis characterization
英文摘要Zeolite Mazzite (MAZ) analogue was synthesized directly using piperazine as a structure directing agent. The reactive gel composition used was (5.0-7.0) piperazine:(6.0-7.0) Na2O:Al2O3:20.0SiO(2):400H(2)O. Using this composition, the reaction time was shortened greatly to 4 days and the crystallization time was reduced as well. The DTA data showed that piperazine, in as-synthesized zeolite omega decomposed easily. The decomposition of the piperazine occurred at 400-480 degrees C. NH3-TPD analysis proved that zeolite H-omega from piperazine had strong surface acidity with ammonia desorption temperature up to 590 degrees C.
WOS标题词Science & Technology ; Physical Sciences ; Technology
类目[WOS]Chemistry, Applied ; Chemistry, Physical ; Materials Science, Multidisciplinary
研究领域[WOS]Chemistry ; Materials Science
关键词[WOS]DIRECTING AGENTS ; N-HEXANE ; OMEGA
收录类别SCI
语种英语
WOS记录号WOS:000247429200013
公开日期2015-08-18
内容类型期刊论文
源URL[http://ir.wipm.ac.cn/handle/112942/4879]  
专题武汉物理与数学研究所_2011年以前论文发表(包括2011年)
作者单位1.Taiyuan Univ Technol, Res Inst Special Chem, Shanxi 030024, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
3.Chinese Acad Sci, State Key Lab Coal Convers, Inst Coal Chem, Taiyuan 030001, Peoples R China
4.Chinese Acad Sci, Wuhan Inst Phys & Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China
推荐引用方式
GB/T 7714
Xu, H.,Dong, P.,Liu, L.,et al. Synthesis and characterization of zeolite mazzite analogue in Na2O-Al2O3-SiO2-Piperazine-H2O[J]. JOURNAL OF POROUS MATERIALS,2007,14(1):97-101.
APA Xu, H.,Dong, P.,Liu, L.,Wang, J.-G.,Deng, F.,&Dong, J.-X..(2007).Synthesis and characterization of zeolite mazzite analogue in Na2O-Al2O3-SiO2-Piperazine-H2O.JOURNAL OF POROUS MATERIALS,14(1),97-101.
MLA Xu, H.,et al."Synthesis and characterization of zeolite mazzite analogue in Na2O-Al2O3-SiO2-Piperazine-H2O".JOURNAL OF POROUS MATERIALS 14.1(2007):97-101.
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