Synthesis of PbS microcrystals via a hydrothermal process

CORC > 物理研究所 > 物理所公开发表论文 > 期刊论文

	Synthesis of PbS microcrystals via a hydrothermal process
	Wang, SQ ; Pan, AL ; Yin, HY ; He, YP ; Lei, Y ; Xu, ZD ; Zou, BS
刊名	MATERIALS LETTERS
	2006
卷号	60 期号:9-10 页码:1242
关键词	DENDRITIC NANOSTRUCTURES NANOCRYSTALS CRYSTALS GROWTH ROUTE
ISSN号	0167-577X
通讯作者	Zou, BS (reprint author), Chinese Acad Sci, Inst Phys, POB 603, Beijing 100080, Peoples R China.
中文摘要	PbS microcrystals including dendrites, multipods, flowers and cubes were prepared by the reaction of Pb(NO3)(2) or Pb(CH3COO)(2) and thiourea (NH2CSNH2) with acrylaraide (AA) as surfactant through a simple hydrothermal process. The samples are characterized by X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM). Uniform PbS crystals were obtained at the temperature of 130-160 degrees C. It is found that thiourea, acrylamide and reaction temperature play important roles in the shape evolutions of PbS microcrystals. A possible formation mechanism of PbS microcrystals was discussed based on their shape evolutions.
收录类别	SCI
语种	英语
公开日期	2013-09-24
内容类型	期刊论文
源URL	[http://ir.iphy.ac.cn/handle/311004/54455]
专题	物理研究所_物理所公开发表论文_物理所公开发表论文_期刊论文
推荐引用方式 GB/T 7714	Wang, SQ,Pan, AL,Yin, HY,et al. Synthesis of PbS microcrystals via a hydrothermal process[J]. MATERIALS LETTERS,2006,60(9-10):1242.
APA	Wang, SQ.,Pan, AL.,Yin, HY.,He, YP.,Lei, Y.,...&Zou, BS.(2006).Synthesis of PbS microcrystals via a hydrothermal process.MATERIALS LETTERS,60(9-10),1242.
MLA	Wang, SQ,et al."Synthesis of PbS microcrystals via a hydrothermal process".MATERIALS LETTERS 60.9-10(2006):1242.