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Synthesis and characterization of carbon-encapsulated Fe nanoparticles by DC carbon arc plasma
Wei, Zhiqiang1,2; Zhu, Lin2; Qiao, Hongxia1; Yang, Hua2; Xia, Tiandong1; Yan, Pengxun3
刊名Zhenkong Kexue yu Jishu Xuebao/Journal of Vacuum Science and Technology
2008-10-01
卷号28期号:5页码:454-457
关键词Electron microscopy Energy dispersive spectroscopy High resolution transmission electron microscopy Nanoparticles Synthesis (chemical) X ray diffraction Carbon arc Carbon encapsulated fe nanoparticles Carbon-encapsulated Microstructures and properties Preparation Synthesis and characterizations Synthesis techniques X-ray energy dispersive spectroscopy
ISSN号16727126
英文摘要The microstructures and properties of the carbon-encapsulated Fe nano-particles, synthesized by the improved DC carbon arc plasma in argon atmosphere, were characterized with X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), X-ray energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), and high resolution transmission electron microscopy (HRTEM). The results show that the synthesis technique works better than the conventional ones, and that the carbon-encapsulated Fe nano-particles have well-defined core-shell structures, with a crystallized iron-core and onion-like, concentric, hexagonal-structured carbon-shells. The spherical and ellipsoidal shapes of the particles dominate, with a size distribution ranging from 20 nm to 60 nm and an average diameter of 44 nm.
语种中文
出版者Science Press
内容类型期刊论文
源URL[http://ir.lut.edu.cn/handle/2XXMBERH/111902]  
专题理学院
作者单位1.State Key Lab. of Advanced New Non-Ferrous Materials, Lanzhou Univ. of Technol., Lanzhou 730050, China;
2.School of Science, Lanzhou Univ. of Technol., Lanzhou 730050, China;
3.School of Physical Science and Technology, Lanzhou University, Lanzhou 730000, China
推荐引用方式
GB/T 7714
Wei, Zhiqiang,Zhu, Lin,Qiao, Hongxia,et al. Synthesis and characterization of carbon-encapsulated Fe nanoparticles by DC carbon arc plasma[J]. Zhenkong Kexue yu Jishu Xuebao/Journal of Vacuum Science and Technology,2008,28(5):454-457.
APA Wei, Zhiqiang,Zhu, Lin,Qiao, Hongxia,Yang, Hua,Xia, Tiandong,&Yan, Pengxun.(2008).Synthesis and characterization of carbon-encapsulated Fe nanoparticles by DC carbon arc plasma.Zhenkong Kexue yu Jishu Xuebao/Journal of Vacuum Science and Technology,28(5),454-457.
MLA Wei, Zhiqiang,et al."Synthesis and characterization of carbon-encapsulated Fe nanoparticles by DC carbon arc plasma".Zhenkong Kexue yu Jishu Xuebao/Journal of Vacuum Science and Technology 28.5(2008):454-457.
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