Preparation and characterization of the cobalt ferrite nano-particles by reverse coprecipitation

doi:10.1016/j.jmmm.2013.12.033

CORC > 兰州理工大学 > 兰州理工大学 > 石油化工学院

	Preparation and characterization of the cobalt ferrite nano-particles by reverse coprecipitation
	Feng Huixia; Chen Baiyi; Zhang Deyi; Zhang Jianqiang; Tan Lin
刊名	JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS
	2014-04
卷号	356 页码:68-72
关键词	Cobalt ferrite nano-particle Reverse coprecipitation method Magnetic property
ISSN号	0304-8853
DOI	10.1016/j.jmmm.2013.12.033
英文摘要	In this paper, cobalt ferrite nano-particles were rapidly prepared using a reverse coprecipitation method. The effects of pH value, aging time, aging temperature and calcination temperature were studied by VSM. XRD and TEM. The results presented that the conditions to obtain the cobalt ferrite nano-particles with a perfect cubic spinel ferrite type structure are the pH value of 12.00, aging time of 60 min, aging temperature of 92 degrees C and calcination temperature of 800 degrees C. The crystallite size of cobalt ferrite increased with increasing the aging and calcination temperature. The saturation magnetization of cobalt ferrite increased with increasing the aging and calcination temperature. The VSM analysis demonstrated that the optimum sample has a high saturation magnetization and proper coercivity, 72.95 emu/g and 717 Oe, respectively. Furthermore, the particle size estimated from the TEM was seen to be larger than that observed from the XRD analysis. Crown Copyright (C) 2013 Published by Elsevier B.V. All rights reserved
资助项目	National Natural Science Foundation of China[51063003] ; Ministry of science and technology project[2009GJG10041] ; Fundamental Research Funds for the Universities of Gansu[1105ZTC136]
WOS研究方向	Materials Science ; Physics
语种	英语
出版者	ELSEVIER
WOS记录号	WOS:000331621700009
状态	已发表
内容类型	期刊论文
源URL	[http://119.78.100.223/handle/2XXMBERH/34414]
专题	石油化工学院教务处（创新创业学院）
通讯作者	Feng Huixia
作者单位	Lanzhou Univ Technol, Coll Petrochem Technol, Lanzhou 730050, Peoples R China
推荐引用方式 GB/T 7714	Feng Huixia,Chen Baiyi,Zhang Deyi,et al. Preparation and characterization of the cobalt ferrite nano-particles by reverse coprecipitation[J]. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS,2014,356:68-72.
APA	Feng Huixia,Chen Baiyi,Zhang Deyi,Zhang Jianqiang,&Tan Lin.(2014).Preparation and characterization of the cobalt ferrite nano-particles by reverse coprecipitation.JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS,356,68-72.
MLA	Feng Huixia,et al."Preparation and characterization of the cobalt ferrite nano-particles by reverse coprecipitation".JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS 356(2014):68-72.