One-pot method fabrication of superparamagnetic sulfonated polystyrene/Fe3O4/graphene oxide micro-nano composites

doi:10.1007/s10934-018-0557-8

	One-pot method fabrication of superparamagnetic sulfonated polystyrene/Fe3O4/graphene oxide micro-nano composites
	Ma, Yingxia; Jin, Pengsheng; Lei, Wenjuan; La, Peiqing; Du, Xueyan; Zhang, Dingjun
刊名	JOURNAL OF POROUS MATERIALS
	2018-10
卷号	25 期号:5 页码:1447-1453
关键词	Sulfonated polystyrene Fe3O4 nanoparticles Graphene oxide One-pot method Micro-nano composites
ISSN号	1380-2224
DOI	10.1007/s10934-018-0557-8
英文摘要	In this work, using monodispersed sulfonated polystyrene (SPS) microspheres as carriers, FeCl3 center dot 6H(2)O and FeSO4 center dot 7H(2)O as precursors, NaOH as precipitant in the presence of graphene oxide (GO), SPS/Fe3O4/GO micro-nano composites were fabricated by a simple one-pot method employing an inverse coprecipitation in-situ compound technology. The SPS/Fe3O4/GO micro-nano composites were characterized by scanning electron microscopy, transmission electron microscopy, X-ray powder diffractometer, Fourier transform infrared spectroscopy, nitrogen adsorption/desorption isotherms and vibrating sample magnetometer. The results show that the SPS/Fe3O4/GO micro-nano composites were fabricated with SPS as core, GO and Fe3O4 nanoparticles as shell. The SPS/Fe3O4/GO micro-nano composites had larger BET specific surface area, average pore width and micropore volume than the pure SPS microspheres. Meanwhile, the SPS/Fe3O4/GO micro-nano composites had superparamagnetism and hydrophilic property. The saturation magnetization (M-s) of the SPS/Fe3O4/GO micro-nano composites was 10.86 emu/g, which was enough to ensure the convenient magnetic separation of solid and liquid phase.
资助项目	National Natural Science Foundation of China[51403091][51663013] ; Postdoctoral Science Foundation of China[2015M572616]
WOS研究方向	Chemistry ; Materials Science
语种	英语
出版者	SPRINGER
WOS记录号	WOS:000439747500020
状态	已发表
内容类型	期刊论文
源URL	[http://119.78.100.223/handle/2XXMBERH/32411]
专题	材料科学与工程学院省部共建有色金属先进加工与再利用国家重点实验室研究生院
通讯作者	Ma, Yingxia
作者单位	Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Sch Mat Sci & Engn, Lanzhou 730050, Gansu, Peoples R China
推荐引用方式 GB/T 7714	Ma, Yingxia,Jin, Pengsheng,Lei, Wenjuan,et al. One-pot method fabrication of superparamagnetic sulfonated polystyrene/Fe3O4/graphene oxide micro-nano composites[J]. JOURNAL OF POROUS MATERIALS,2018,25(5):1447-1453.
APA	Ma, Yingxia,Jin, Pengsheng,Lei, Wenjuan,La, Peiqing,Du, Xueyan,&Zhang, Dingjun.(2018).One-pot method fabrication of superparamagnetic sulfonated polystyrene/Fe3O4/graphene oxide micro-nano composites.JOURNAL OF POROUS MATERIALS,25(5),1447-1453.
MLA	Ma, Yingxia,et al."One-pot method fabrication of superparamagnetic sulfonated polystyrene/Fe3O4/graphene oxide micro-nano composites".JOURNAL OF POROUS MATERIALS 25.5(2018):1447-1453.