Preparation and characterization of a new reference standard GSB-Mg for Mg isotopic analysis
Bao, Zhian4; Huang, Kang-Jun4; Xu, Juan3; Deng, Li2; Yang, Shufeng1; Zhang, Pan4; Yuan, Honglin4
刊名JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY
2020-06-01
卷号35期号:6页码:1080-1086
ISSN号0267-9477
DOI10.1039/d0ja00059k
英文摘要

We have prepared a large volume of pure, concentrated and homogeneous magnesium standard solution (GSB-Mg) to be used as a secondary reference standard by the magnesium isotope community. This new standard solution can also be used for quality assurance, including the development and validation of analytical procedures, preparation and test of analytical methods, quality control and training of analysts. The delta Mg-26 values relative to DSM3, measured by multiple-collector inductively coupled plasma mass spectrometry (MC-ICP-MS), are -2.038 +/- 0.027 parts per thousand (n= 45, Lab 1), -2.024 +/- 0.055 parts per thousand (n= 7, Lab 2), -2.078 +/- 0.081 parts per thousand (n= 6, Lab 3), -2.037 +/- 0.015 parts per thousand (n= 8, Lab 4), and -2.067 +/- 0.039 parts per thousand (n= 12, Lab 5). The delta Mg-26 and delta Mg-25 values for the GSB-Mg standard solution are -2.049 parts per thousand and -1.056 parts per thousand, with a combined expanded (k= 2) uncertainty of 0.049 parts per thousand and 0.028 parts per thousand, respectively. These values show higher similarity to Mg isotopic compositions of carbonates and marine sediments compared to those of the mantle and crustal rocks, making the GSB-Mg solution a great reference material for Mg isotopic analysis of carbonates and marine sediments.

资助项目National Natural Science Foundation of China[41825007] ; National Natural Science Foundation of China[41421002] ; National Natural Science Foundation of China[41973008] ; National Natural Science Foundation of China[41703027] ; National Natural Science Foundation of China[41890845] ; MOST Research Foundation from the State Key Laboratory of Continental Dynamics[207010021]
WOS关键词MAGNESIUM ; FRACTIONATION ; GEOCHEMISTRY ; OLIVINE ; CALCITE ; ROCKS
WOS研究方向Chemistry ; Spectroscopy
语种英语
出版者ROYAL SOC CHEMISTRY
WOS记录号WOS:000544032100005
资助机构National Natural Science Foundation of China ; MOST Research Foundation from the State Key Laboratory of Continental Dynamics
内容类型期刊论文
源URL[http://ir.ieecas.cn/handle/361006/15034]  
专题地球环境研究所_加速器质谱中心
通讯作者Yuan, Honglin
作者单位1.Lanzhou Univ, Sch Earth Sci, Key Lab Western Chinas Mineral Resource Gansu Pro, Lanzhou 730000, Peoples R China
2.Chinese Acad Sci, Inst Earth Environm, State Key Lab Loess & Quaternary Geol, Xian 710061, Peoples R China
3.Tongji Univ, State Key Lab Marine Geol, Shanghai 200092, Peoples R China
4.Northwest Univ, Dept Geol, State Key Lab Continental Dynam, Xian 710069, Peoples R China
推荐引用方式
GB/T 7714
Bao, Zhian,Huang, Kang-Jun,Xu, Juan,et al. Preparation and characterization of a new reference standard GSB-Mg for Mg isotopic analysis[J]. JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY,2020,35(6):1080-1086.
APA Bao, Zhian.,Huang, Kang-Jun.,Xu, Juan.,Deng, Li.,Yang, Shufeng.,...&Yuan, Honglin.(2020).Preparation and characterization of a new reference standard GSB-Mg for Mg isotopic analysis.JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY,35(6),1080-1086.
MLA Bao, Zhian,et al."Preparation and characterization of a new reference standard GSB-Mg for Mg isotopic analysis".JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY 35.6(2020):1080-1086.
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