The major trap sites of deuterium in CuCrZr alloy | |
Liu, Hao-Dong1; Zhou, Hai-Shan1; Zhao, Si-Xiang3; Wang, Lu1,2; Wei, Ran1,2; Luo, Guang-Nan1,2 | |
刊名 | NUCLEAR MATERIALS AND ENERGY |
2020-05-01 | |
卷号 | 23 |
关键词 | Heat treatment Hydrogen isotope Retention CuCrZr alloy |
DOI | 10.1016/j.nme.2020.100755 |
通讯作者 | Zhou, Hai-Shan(haishanzhou@ipp.ac.cn) |
英文摘要 | The energy characteristics of the main deuterium (D) traps in CuCrZr alloy samples, which were previously annealed at temperatures of 773, 873, 973 and 1073 K and then exposed to D2 gas at a pressure of 2.5 x 104 Pa and a temperature of 723 K for 10 h, were studied by thermal desorption spectroscopy. Samples of oxygen free copper (OFC) were also investigated in the same way. For OFC, annealing at 773 K could reduce D retention appreciably. It indicates the temperature of 773 K is high enough to reduce the total D amount trapped by intrinsic defects (i.e. vacancies, dislocations and grain boundaries). However, for CuCrZr alloy, heat treatment does not reduce the D retention significantly until the annealing temperature is higher than 1073 K. Scanning electron microscope (SEM) and energy dispersive spectrometer (EDS) observations show that the density of precipitate particles especially the Zr-rich precipitate particles increase for the 1073 K-annealed one. It suggests the dissolved Zr atoms in the substrate are responsible for the D retention in CuCrZr alloy. D detrapping energy from the dissolved Zr atoms in CuCrZr alloy is estimated to be 0.98 eV from the TDS measurements. |
资助项目 | National Key R&D Program of China[2017YFE0301502] ; National Natural Science Foundation of China[11875288] ; National Natural Science Foundation of China[11705232] ; Users with Excellence Project of Hefei Science Center CAS[2018HSC-UE006] ; Youth Innovation Promotion Association CAS[2018484] |
WOS关键词 | HEAT-TREATMENTS ; MICROSTRUCTURE ; RETENTION |
WOS研究方向 | Nuclear Science & Technology |
语种 | 英语 |
出版者 | ELSEVIER |
WOS记录号 | WOS:000569101000006 |
资助机构 | National Key R&D Program of China ; National Natural Science Foundation of China ; Users with Excellence Project of Hefei Science Center CAS ; Youth Innovation Promotion Association CAS |
内容类型 | 期刊论文 |
源URL | [http://ir.hfcas.ac.cn:8080/handle/334002/104133] |
专题 | 中国科学院合肥物质科学研究院 |
通讯作者 | Zhou, Hai-Shan |
作者单位 | 1.Chinese Acad Sci, Inst Plasma Phys, Hefei 230031, Anhui, Peoples R China 2.Univ Sci & Technol China, Sci Isl Branch, Grad Sch, Hefei 230031, Anhui, Peoples R China 3.Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Lanzhou 730050, Gansu, Peoples R China |
推荐引用方式 GB/T 7714 | Liu, Hao-Dong,Zhou, Hai-Shan,Zhao, Si-Xiang,et al. The major trap sites of deuterium in CuCrZr alloy[J]. NUCLEAR MATERIALS AND ENERGY,2020,23. |
APA | Liu, Hao-Dong,Zhou, Hai-Shan,Zhao, Si-Xiang,Wang, Lu,Wei, Ran,&Luo, Guang-Nan.(2020).The major trap sites of deuterium in CuCrZr alloy.NUCLEAR MATERIALS AND ENERGY,23. |
MLA | Liu, Hao-Dong,et al."The major trap sites of deuterium in CuCrZr alloy".NUCLEAR MATERIALS AND ENERGY 23(2020). |
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