Liquid precursor-derived high-entropy carbide nanopowders
Li, Fei; Lu, Ying; Wang, Xin-Gang; Bao, Weichao; Liu, Ji-Xuan; Xu, Fangfang; Zhang, Guo-Jun
刊名CERAMICS INTERNATIONAL
2019-12-01
卷号45期号:17页码:22437
关键词Precursor-derived ceramics High-entropy materials Transition metal carbide Nanopowders
ISSN号0272-8842
DOI10.1016/j.ceramint.2019.07.244
文献子类Article
英文摘要We report a simple liquid precursor method for the synthesis of single-phase high-entropy carbide (HEC) nanopowders. Transition metal halides (TiCl4, ZrCl4, HfCl4, NbCl5, TaCl5) and furfuryl alcohol are used as metal sources and carbon source. The liquid precursor can be converted into mixtures of five binary carbides via carbothermal reduction at 1400 degrees C in vacuum, and can be further transformed into single-phase HEC nanopowders through solid solution formation by heat treatment at 2000 degrees C. The as-synthesized HEC nanopowders possess an average particle size of 132 +/- 5 nm, a specific surface area of 24.5 m(2)/g, and an oxygen content of 0.22 wt%, respectively.
WOS研究方向Materials Science
语种英语
出版者ELSEVIER SCI LTD
内容类型期刊论文
源URL[http://ir.sic.ac.cn/handle/331005/26697]  
专题中国科学院上海硅酸盐研究所
推荐引用方式
GB/T 7714
Li, Fei,Lu, Ying,Wang, Xin-Gang,et al. Liquid precursor-derived high-entropy carbide nanopowders[J]. CERAMICS INTERNATIONAL,2019,45(17):22437.
APA Li, Fei.,Lu, Ying.,Wang, Xin-Gang.,Bao, Weichao.,Liu, Ji-Xuan.,...&Zhang, Guo-Jun.(2019).Liquid precursor-derived high-entropy carbide nanopowders.CERAMICS INTERNATIONAL,45(17),22437.
MLA Li, Fei,et al."Liquid precursor-derived high-entropy carbide nanopowders".CERAMICS INTERNATIONAL 45.17(2019):22437.
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