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The Formation and Utility of Sub-Angstrom to Nanometer-Sized Electron Probes in the Aberration-Corrected Transmission Electron Microscope at the University of Illinois
Wen, Jianguo ; Mabon, James ; Lei, Changhui ; Burdin, Steve ; Sammann, Ernie ; Petrov, Ivan ; Shah, Arnish B. ; Chobpattana, Varistha ; Zhang, Jiong ; Ran, Ke ; Zuo, Jian-Min ; Mishina, Satoshi ; Aoki, Toshihiro
刊名microscopy and microanalysis
2010
关键词aberration-corrected scanning transmission electron microscopy high-angle annular dark-field imaging electron energy loss spectroscopy nanobeam diffraction aperture nanobeam diffraction STEM DIFFRACTION NANOCRYSTALS PERFORMANCE CRYSTALS
DOI10.1017/S1431927610000085
英文摘要We evaluate the probe forming capability of a JEOL 2200FS transmission electron microscope equipped with a spherical aberration (C(s)) probe corrector. The achievement of a real space sub-Angstrom (0.1 nm) probe for scanning transmission electron microscopy (STEM) imaging is demonstrated by acquisition and modeling of high-angle annular dark-field STEM images. We show that by optimizing the illumination system, large probe currents and large collection angles for electron energy loss spectroscopy (EELS) can be combined to yield EELS fine structure data spatially resolved to the atomic scale. We demonstrate the probe forming flexibility provided by the additional lenses in the probe corrector in several ways, including the formation of nanometer-sized parallel beams for nanoarea electron diffraction, and the formation of focused probes for convergent beam electron diffraction with a range of convergence angles. The different probes that can be formed using the probe corrected STEM opens up new applications for electron microscopy and diffraction.; Materials Science, Multidisciplinary; Microscopy; SCI(E); 21; ARTICLE; 2; 183-193; 16
语种英语
内容类型期刊论文
源URL[http://ir.pku.edu.cn/handle/20.500.11897/395857]  
专题信息科学技术学院
推荐引用方式
GB/T 7714
Wen, Jianguo,Mabon, James,Lei, Changhui,et al. The Formation and Utility of Sub-Angstrom to Nanometer-Sized Electron Probes in the Aberration-Corrected Transmission Electron Microscope at the University of Illinois[J]. microscopy and microanalysis,2010.
APA Wen, Jianguo.,Mabon, James.,Lei, Changhui.,Burdin, Steve.,Sammann, Ernie.,...&Aoki, Toshihiro.(2010).The Formation and Utility of Sub-Angstrom to Nanometer-Sized Electron Probes in the Aberration-Corrected Transmission Electron Microscope at the University of Illinois.microscopy and microanalysis.
MLA Wen, Jianguo,et al."The Formation and Utility of Sub-Angstrom to Nanometer-Sized Electron Probes in the Aberration-Corrected Transmission Electron Microscope at the University of Illinois".microscopy and microanalysis (2010).
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