ANALYSIS OF C-60 AND C-70 FULLERENES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY | |
WU, YQ ; SUN, YL ; GU, ZN ; WANG, QW ; ZHOU, XH ; XIONG, Y ; JIN, ZX | |
刊名 | journal of chromatography |
1993 | |
关键词 | BUCKMINSTERFULLERENE C60 PURIFICATION SEPARATION CLUSTERS PHASES DACC C70 GEL |
DOI | 10.1016/0021-9673(93)80434-A |
英文摘要 | Some common solvents were roughly classified into four classes according to their decreasing solubility for fullerenes. Good solvents should be used in designing a practical liquid chromatographic separation method. Several stationary phases were tested to separate C60 and C70 fullerenes. They included ODS-, C6H5-, NH2- and CN-silica, silica gel and three synthesized ones containing mono-/di- nitrobenzamidopropyl functionalities. All the stationary phases studied, with the exception of silica gel, had some retention and separation capability for C60 and C70 fullerenes. The three nitrobenzamidopropyl group-containing packings showed more pronounced retention and were capable of being used with good solvent added in the mobile phase. 3,5-Dinitrobenzamidopropyl chemically bonded phase, the most retentive packing, was used as stationary phase in HPLC for the analysis of C60 and C70 fullerenes. It was shown that with toluene-light petroleum as mobile phase this method was rapid and accurate.; Chemistry, Analytical; SCI(E); 21; NOTE; 2; 491-496; 648 |
语种 | 英语 |
内容类型 | 期刊论文 |
源URL | [http://ir.pku.edu.cn/handle/20.500.11897/402173] |
专题 | 化学与分子工程学院 |
推荐引用方式 GB/T 7714 | WU, YQ,SUN, YL,GU, ZN,et al. ANALYSIS OF C-60 AND C-70 FULLERENES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY[J]. journal of chromatography,1993. |
APA | WU, YQ.,SUN, YL.,GU, ZN.,WANG, QW.,ZHOU, XH.,...&JIN, ZX.(1993).ANALYSIS OF C-60 AND C-70 FULLERENES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY.journal of chromatography. |
MLA | WU, YQ,et al."ANALYSIS OF C-60 AND C-70 FULLERENES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY".journal of chromatography (1993). |
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