单颗粒-电感耦合等离子体质谱测定金纳米颗粒 | |
罗瑞平; 郑令娜; 丰伟悦; 王萌; Luo, RP; Zheng, LN; Li, L; Wang, J; Feng, WY; Yu, XH | |
刊名 | 分析化学 |
2018 | |
卷号 | 46期号:6页码:925-930 |
关键词 | Gold nanoparticles Single particle inductively coupled plasma mass spectrometry Dwell time Settling time |
ISSN号 | 0253-3820 |
DOI | 10.11895/j.issn.0253.3820.181059 |
其他题名 | Effect of Data Acquisition Parameters on Characterization of Gold Nanoparticles By Single Particle Inductively Coupled Plasma-Mass Spectrometry |
文献子类 | Article |
英文摘要 | Single particle inductively coupled plasma mass spectrometry (SP-ICP-MS) is a new tool that can provide the element composition, size distribution, and number concentration of nanoparticles. Here we discussed the effects of dwell time and settling time on analysis of nanoparticles by SP-ICP-MS. We analyzed standard materials of gold nanoparticles (30, 40 and 60 nm AuNPs, from NIST and NCNST), showing that better signal. to. noise ratio and higher determination efficiency could be achived when using shorter dwell time and settling time. We utilized a nano mode for SP-ICP-MS, in which the dwell time was set as 0.05 ms and the settling time was 0. The size of NIST AuNP standard material determined here was in accord with the certified size using the developed method. The detection limits of size and number concentration of AuNPs were 8 nm and 1.1 x 10(5) particle/L, respectively. |
电子版国际标准刊号 | 1872-2040 |
WOS关键词 | ICP-MS ; COLLOID ANALYSIS ; TRANSPORT ; SILVER ; CELLS |
WOS研究方向 | Chemistry |
语种 | 中文 |
CSCD记录号 | CSCD:6254188 |
WOS记录号 | WOS:000455903900012 |
内容类型 | 期刊论文 |
源URL | [http://ir.ihep.ac.cn/handle/311005/286974] |
专题 | 高能物理研究所_多学科研究中心 |
通讯作者 | 王萌 |
作者单位 | 中国科学院高能物理研究所 |
推荐引用方式 GB/T 7714 | 罗瑞平,郑令娜,丰伟悦,等. 单颗粒-电感耦合等离子体质谱测定金纳米颗粒[J]. 分析化学,2018,46(6):925-930. |
APA | 罗瑞平.,郑令娜.,丰伟悦.,王萌.,Luo, RP.,...&Wang, M.(2018).单颗粒-电感耦合等离子体质谱测定金纳米颗粒.分析化学,46(6),925-930. |
MLA | 罗瑞平,et al."单颗粒-电感耦合等离子体质谱测定金纳米颗粒".分析化学 46.6(2018):925-930. |
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