单颗粒-电感耦合等离子体质谱测定金纳米颗粒
罗瑞平; 郑令娜; 丰伟悦; 王萌; Luo, RP; Zheng, LN; Li, L; Wang, J; Feng, WY; Yu, XH
刊名分析化学
2018
卷号46期号:6页码:925-930
关键词Gold nanoparticles Single particle inductively coupled plasma mass spectrometry Dwell time Settling time
ISSN号0253-3820
DOI10.11895/j.issn.0253.3820.181059
其他题名Effect of Data Acquisition Parameters on Characterization of Gold Nanoparticles By Single Particle Inductively Coupled Plasma-Mass Spectrometry
文献子类Article
英文摘要Single particle inductively coupled plasma mass spectrometry (SP-ICP-MS) is a new tool that can provide the element composition, size distribution, and number concentration of nanoparticles. Here we discussed the effects of dwell time and settling time on analysis of nanoparticles by SP-ICP-MS. We analyzed standard materials of gold nanoparticles (30, 40 and 60 nm AuNPs, from NIST and NCNST), showing that better signal. to. noise ratio and higher determination efficiency could be achived when using shorter dwell time and settling time. We utilized a nano mode for SP-ICP-MS, in which the dwell time was set as 0.05 ms and the settling time was 0. The size of NIST AuNP standard material determined here was in accord with the certified size using the developed method. The detection limits of size and number concentration of AuNPs were 8 nm and 1.1 x 10(5) particle/L, respectively.
电子版国际标准刊号1872-2040
WOS关键词ICP-MS ; COLLOID ANALYSIS ; TRANSPORT ; SILVER ; CELLS
WOS研究方向Chemistry
语种中文
CSCD记录号CSCD:6254188
WOS记录号WOS:000455903900012
内容类型期刊论文
源URL[http://ir.ihep.ac.cn/handle/311005/286974]  
专题高能物理研究所_多学科研究中心
通讯作者王萌
作者单位中国科学院高能物理研究所
推荐引用方式
GB/T 7714
罗瑞平,郑令娜,丰伟悦,等. 单颗粒-电感耦合等离子体质谱测定金纳米颗粒[J]. 分析化学,2018,46(6):925-930.
APA 罗瑞平.,郑令娜.,丰伟悦.,王萌.,Luo, RP.,...&Wang, M.(2018).单颗粒-电感耦合等离子体质谱测定金纳米颗粒.分析化学,46(6),925-930.
MLA 罗瑞平,et al."单颗粒-电感耦合等离子体质谱测定金纳米颗粒".分析化学 46.6(2018):925-930.
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