Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method | |
Yan, SF; Ling, W; Zhou, EL | |
刊名 | JOURNAL OF CRYSTAL GROWTH |
2004-12-17 | |
卷号 | 273期号:1-2页码:226-233 |
关键词 | Crystallites Crystal Structure X-ray Diffraction Nanomaterials |
ISSN号 | 0022-0248 |
DOI | 10.1016/j.jcrysgro.2004.08.025 |
英文摘要 | MnZn-ferrite/SiO2 nanocomposites with different silica content were successfully fabricated by a novel modified sol-gel auto-combustion method using citric acid as a chelating agent and tetraethyl orthosilicate (TEOS) as the source of silica matrix. The auto-combustion nature of the dried gel was studied by X-ray diffraction (XRD), Infrared spectra (IR), thermogravimetry (TG) and differential thermal analysis (DTA). Transmission electron microscope (TEM) observation shows that the MnZn-ferrite particles are homogeneously dispersed in silica matrix after auto-combustion of the dried gels. The magnetic properties vary with the silica content. The transition from the ferromagnetic to paramagnetic state is observed by Mossbauer spectra measurement with the increasing silica content. Vibrating sample magnetometer (VSM) shows that the magnetic properties of Mn0.65Zn0.35Fe2O4/SiO2 nanocomposites strongly depend on the silica content. (C) 2004 Elsevier B.V. All rights reserved. |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE BV |
WOS记录号 | WOS:000226021000030 |
内容类型 | 期刊论文 |
源URL | [http://ir.iccas.ac.cn/handle/121111/55155] |
专题 | 中国科学院化学研究所 |
通讯作者 | Zhou, EL |
作者单位 | Chinese Acad Sci, Grad Sch, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China |
推荐引用方式 GB/T 7714 | Yan, SF,Ling, W,Zhou, EL. Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method[J]. JOURNAL OF CRYSTAL GROWTH,2004,273(1-2):226-233. |
APA | Yan, SF,Ling, W,&Zhou, EL.(2004).Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method.JOURNAL OF CRYSTAL GROWTH,273(1-2),226-233. |
MLA | Yan, SF,et al."Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method".JOURNAL OF CRYSTAL GROWTH 273.1-2(2004):226-233. |
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