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Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method
Yan, SF; Ling, W; Zhou, EL
刊名JOURNAL OF CRYSTAL GROWTH
2004-12-17
卷号273期号:1-2页码:226-233
关键词Crystallites Crystal Structure X-ray Diffraction Nanomaterials
ISSN号0022-0248
DOI10.1016/j.jcrysgro.2004.08.025
英文摘要MnZn-ferrite/SiO2 nanocomposites with different silica content were successfully fabricated by a novel modified sol-gel auto-combustion method using citric acid as a chelating agent and tetraethyl orthosilicate (TEOS) as the source of silica matrix. The auto-combustion nature of the dried gel was studied by X-ray diffraction (XRD), Infrared spectra (IR), thermogravimetry (TG) and differential thermal analysis (DTA). Transmission electron microscope (TEM) observation shows that the MnZn-ferrite particles are homogeneously dispersed in silica matrix after auto-combustion of the dried gels. The magnetic properties vary with the silica content. The transition from the ferromagnetic to paramagnetic state is observed by Mossbauer spectra measurement with the increasing silica content. Vibrating sample magnetometer (VSM) shows that the magnetic properties of Mn0.65Zn0.35Fe2O4/SiO2 nanocomposites strongly depend on the silica content. (C) 2004 Elsevier B.V. All rights reserved.
语种英语
出版者ELSEVIER SCIENCE BV
WOS记录号WOS:000226021000030
内容类型期刊论文
源URL[http://ir.iccas.ac.cn/handle/121111/55155]  
专题中国科学院化学研究所
通讯作者Zhou, EL
作者单位Chinese Acad Sci, Grad Sch, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China
推荐引用方式
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Yan, SF,Ling, W,Zhou, EL. Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method[J]. JOURNAL OF CRYSTAL GROWTH,2004,273(1-2):226-233.
APA Yan, SF,Ling, W,&Zhou, EL.(2004).Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method.JOURNAL OF CRYSTAL GROWTH,273(1-2),226-233.
MLA Yan, SF,et al."Rapid synthesis of Mn0.65Zn0.35Fe2O4/SiO2 homogeneous nanocomposites by modified sol-gel auto-combustion method".JOURNAL OF CRYSTAL GROWTH 273.1-2(2004):226-233.
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