Preparation and characterization of hydrogenated carbon nitride films synthesized by dual dc-rf plasma system | |
Hao, JY; Xu, T; Liu, WM | |
刊名 | Materials science and engineering a-structural materials properties microstructure and processing |
2005-11-05 | |
卷号 | 408期号:1-2页码:297-302 |
关键词 | Carbon nitride films Pecvd Composition Mechanical properties |
ISSN号 | 0921-5093 |
DOI | 10.1016/j.msea.2005.08.146 |
通讯作者 | Liu, wm() |
英文摘要 | Carbon nitride films (cnx films) were deposited on si(100) substrates making use of dual direct current radio frequency (dc-rf) plasma enhanced chemical vapor deposition (pecvd), using a mixed gas of ch4 and n-2 as the source gas. the microstructures, morphologies, and compositions of the resulting cnx films were analyzed by means of atomic force microscopy (afm), transmission electron microscopy (tem), xray photoelectron spectroscopy (xps), fourier transformation infrared spectrometry (ftir), and raman spectroscopy. the mechanical properties of the cnx films were examined using a nano-indentation test system. the raman spectrum showed two characteristic bands: a graphite g band and a disordered d band of carbon, which suggested the presence of an amorphous carbon matrix. ftir and xps measurements suggested the existence of c-nh, c=nh, c&3bond; n, n-h, and c-h in the cnx films, and the nitrogen to carbon atom ratio (n/c) is as much as 0.50. moreover, the tem showed various diffraction rings of different d values, which could confirm the polycrystallites embedded in the cnx matrix. besides, the quality and elasticity of the cnx films were significantly improved by the incorporation of nitrogen. the films prepared in the present work had much higher hardness and young's modulus than the dlc films prepared under the same conditions, and the elastic recovery parameter was up to 89%. (c) 2005 elsevier b.v. all rights reserved. |
WOS关键词 | CHEMICAL-VAPOR-DEPOSITION ; DIAMOND-LIKE CARBON ; AMORPHOUS-CARBON ; THIN-FILMS ; MECHANICAL-PROPERTIES ; INFRARED-ABSORPTION ; ION ; RESONANCE ; RAMAN ; XPS |
WOS研究方向 | Science & Technology - Other Topics ; Materials Science ; Metallurgy & Metallurgical Engineering |
WOS类目 | Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE SA |
WOS记录号 | WOS:000233524700042 |
内容类型 | 期刊论文 |
URI标识 | http://www.corc.org.cn/handle/1471x/2377850 |
专题 | 中国科学院大学 |
通讯作者 | Liu, WM |
作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Solid Lubricat, Lanzhou 730000, Peoples R China 2.Grad Univ, Chinese Acad Sci, Beijing 100039, Peoples R China |
推荐引用方式 GB/T 7714 | Hao, JY,Xu, T,Liu, WM. Preparation and characterization of hydrogenated carbon nitride films synthesized by dual dc-rf plasma system[J]. Materials science and engineering a-structural materials properties microstructure and processing,2005,408(1-2):297-302. |
APA | Hao, JY,Xu, T,&Liu, WM.(2005).Preparation and characterization of hydrogenated carbon nitride films synthesized by dual dc-rf plasma system.Materials science and engineering a-structural materials properties microstructure and processing,408(1-2),297-302. |
MLA | Hao, JY,et al."Preparation and characterization of hydrogenated carbon nitride films synthesized by dual dc-rf plasma system".Materials science and engineering a-structural materials properties microstructure and processing 408.1-2(2005):297-302. |
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