Preparation of superparamagnetic maghemite (gamma-fe2o3) nanoparticles by wet chemical route and investigation of their magnetic and dielectric properties | |
Ali, Kashif1; Sarfraz, A. K.1; Mirza, Imran M.1; Bahadur, A.1,2; Iqbal, S.2; ul Haq, A.3 | |
刊名 | Current applied physics |
2015-08-01 | |
卷号 | 15期号:8页码:925-929 |
关键词 | Superparamagnetic maghemite (gamma-fe2o3) nanoparticles Wet chemical method Xrd measurements Dielectric constant and tangent losses M-h and m-t loop |
ISSN号 | 1567-1739 |
DOI | 10.1016/j.cap.2015.04.030 |
通讯作者 | Sarfraz, a. k.(sakqau1@gmail.com) |
英文摘要 | Maghemite (gamma-fe2o3) nanoparticles have been synthesized using a wet chemical route, optimizing the reaction time, ph value and size of the crystallite during synthesis. the powder x-ray diffraction (xrd) measurements confirmed the presence of an impurity free maghemite phase in our sample with an average crystallite size of 16 nm as calculated from the debye-scherrer equation. in physical characterization, the room temperature hysteresis (m-h loop) and blocking temperature (as observed from the m-t plot) revealed that the particles are in the superparamagnetic phase at room temperature. dielectric behaviour of gamma-fe2o3 with respect to the variation of frequency and temperature was also performed. at room temperatures, we observe a decaying behaviour of both dielectric constant (epsilon) and tangent looses (tan delta) at smaller frequencies while at higher frequencies both saturate to smaller constant values. in temperature dependent dielectric properties we notice that the dielectric constant (both real and imaginary parts) show an increasing trend with increasing temperatures but an overall slower enhancement at elevated frequencies. the former effect can be attributed to the possible delocalization of impurities at higher temperatures while the latter effect can be explained as an inability of the electric dipole moments to respond at higher frequencies. (c) 2015 elsevier b.v. all rights reserved. |
WOS关键词 | IRON-OXIDE NANOPARTICLES ; LOW-TEMPERATURE ; SURFACE ; NANOSTRUCTURES ; ALPHA-FE2O3 ; PARTICLES ; FE3O4 ; FILMS ; FIELD ; SIZE |
WOS研究方向 | Materials Science ; Physics |
WOS类目 | Materials Science, Multidisciplinary ; Physics, Applied |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE BV |
WOS记录号 | WOS:000356550400014 |
内容类型 | 期刊论文 |
URI标识 | http://www.corc.org.cn/handle/1471x/2376477 |
专题 | 中国科学院大学 |
通讯作者 | Sarfraz, A. K. |
作者单位 | 1.Quaid I Azam Univ, Islamabad, Pakistan 2.Univ Chinese Acad Sci, Sch Chem & Chem Engn, Beijing 100049, Peoples R China 3.Riphah Int Univ, Islamabad, Pakistan |
推荐引用方式 GB/T 7714 | Ali, Kashif,Sarfraz, A. K.,Mirza, Imran M.,et al. Preparation of superparamagnetic maghemite (gamma-fe2o3) nanoparticles by wet chemical route and investigation of their magnetic and dielectric properties[J]. Current applied physics,2015,15(8):925-929. |
APA | Ali, Kashif,Sarfraz, A. K.,Mirza, Imran M.,Bahadur, A.,Iqbal, S.,&ul Haq, A..(2015).Preparation of superparamagnetic maghemite (gamma-fe2o3) nanoparticles by wet chemical route and investigation of their magnetic and dielectric properties.Current applied physics,15(8),925-929. |
MLA | Ali, Kashif,et al."Preparation of superparamagnetic maghemite (gamma-fe2o3) nanoparticles by wet chemical route and investigation of their magnetic and dielectric properties".Current applied physics 15.8(2015):925-929. |
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