Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process

CORC > 青海盐湖研究所 > 中国科学院青海盐湖研究所 > 青海盐湖研究所知识仓储

	Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process
	Zhu Donghai 1,2; Nai Xueying 2; Lan Shengjie 1,3; Dang Li 1,3; Liu Xin 2; Li Wu 2
刊名	JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
	2017-10-01
卷号	32 期号:5 页码:1067-1071
关键词	Single Crystal Growth Ca2b5o9cl Whiskers Microstructures
文献子类	Article
英文摘要	Single crystalline calcium chloroborate (Ca2B5O9Cl) whiskers with uniform diameter have been fabricated by a two-step process. The precursor was firstly prepared by the sedimentation reaction between CaCl2, H3BO3 and NaOH aqueous solutions, and then sintered at different temperatures for 6 h with KCl as flux. The XRD indicates that the product synthesized at 600 degrees C is Orthorhombic Ca2B5O9Cl. SEM and TEM results show that the Ca2B5O9Cl is whisker with the diameter about 0.2-0.5 mu m and the length up to 15 mu m. SAED analysis shows that the whisker is single crystalline and grows along [001] direction. The possible formation process and growth mechanism were proposed.
WOS关键词	ALUMINUM BORATE WHISKERS ; MECHANICAL-PROPERTIES ; COMPOSITES ; BEHAVIORS
WOS研究方向	Materials Science
语种	英语
WOS记录号	WOS:000412950000013
内容类型	期刊论文
源URL	[http://ir.isl.ac.cn/handle/363002/6261]
专题	青海盐湖研究所_青海盐湖研究所知识仓储青海盐湖研究所_盐湖资源综合利用工程技术中心
作者单位	1.Qinghai Univ, State Key Lab Plateau Ecol & Agr, Xining 810016, Qinghai, Peoples R China 2.Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China 3.Qinghai Univ, Sch Chem Engn, Xining 810016, Qinghai, Peoples R China
推荐引用方式 GB/T 7714	Zhu Donghai,Nai Xueying,Lan Shengjie,et al. Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2017,32(5):1067-1071.
APA	Zhu Donghai,Nai Xueying,Lan Shengjie,Dang Li,Liu Xin,&Li Wu.(2017).Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,32(5),1067-1071.
MLA	Zhu Donghai,et al."Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 32.5(2017):1067-1071.