Synthesis and magnetic properties of nanocrystalline Gd3Fe5O12 and GdFeO3 powders prepared by sol-gel auto-combustion method
Jiang, Linwen1; Yang, Shanshan; Zheng, Mengyao; Chen, Hongbing; Wu, Anhua2
刊名MATERIALS RESEARCH BULLETIN
2018
卷号104页码:92
关键词GdFeO3 Gd3Fe5O12 Auto-combustion method Sol-gel Magnetic properties
ISSN号0025-5408
DOI10.1016/j.materresbull.2018.04.010
英文摘要Nanocrystalline GdFeO3 and Gd3Fe5O12 powders were prepared successfully by sol-gel auto-combustion method using a glycine-based gel. The as-prepared GdFeO3 and Gd3Fe5O12 powders presented spherical shape, and composed of continuous porous network structure due to the releasing of a large amount of gases during auto-combustion process. This special microstructure was significant for reducing the magnetic interactions between nanocrystalline powders. The Gd3Fe5O12 samples presented ferrimagnetic feature at low temperatures. At 10 K, the saturate magnetization is about 87.9 emu/g. As temperature increased to 300 K, the magnetization decreased rapidly since the thermal fluctuations changed the main magnetic spin ordering. The GdFeO3 samples presented antiferromagnetic feature at 5 K, and the magnetization reaches 109 emu/g at 50,000 Oe field. As temperature increased to 300 K, the antiferromagnetism decreased rapidly, and the magnetization curve presents linear tendency due to the dominant paramagnetism contribution of Gd3+ ions.
学科主题Materials Science, Multidisciplinary
出版者PERGAMON-ELSEVIER SCIENCE LTD
WOS记录号WOS:000432769900016
资助机构This work is supported by Natural Science Foundation of China (No. 51701098), and Natural Science Foundation of Ningbo municipality (No. 2017A610100). This work is also sponsored by the Opening Project of State Key laboratory of Crystal Material in Shandong University (KF1706), and K. C. Wong Magna Foundation in Ningbo University. ; This work is supported by Natural Science Foundation of China (No. 51701098), and Natural Science Foundation of Ningbo municipality (No. 2017A610100). This work is also sponsored by the Opening Project of State Key laboratory of Crystal Material in Shandong University (KF1706), and K. C. Wong Magna Foundation in Ningbo University.
内容类型期刊论文
源URL[http://ir.sic.ac.cn/handle/331005/24799]  
专题中国科学院上海硅酸盐研究所
作者单位1.Ningbo Univ, Key Lab Photoelect Detect Mat & Devices Zhejiang, State Key Base Funct Mat & Its Preparat Sci, Ningbo 315211, Zhejiang, Peoples R China
2.Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Shandong, Peoples R China
3.Chinese Acad Sci, Shanghai Inst Ceram, Shanghai 201800, Peoples R China
推荐引用方式
GB/T 7714
Jiang, Linwen,Yang, Shanshan,Zheng, Mengyao,et al. Synthesis and magnetic properties of nanocrystalline Gd3Fe5O12 and GdFeO3 powders prepared by sol-gel auto-combustion method[J]. MATERIALS RESEARCH BULLETIN,2018,104:92, 96.
APA Jiang, Linwen,Yang, Shanshan,Zheng, Mengyao,Chen, Hongbing,&Wu, Anhua.(2018).Synthesis and magnetic properties of nanocrystalline Gd3Fe5O12 and GdFeO3 powders prepared by sol-gel auto-combustion method.MATERIALS RESEARCH BULLETIN,104,92.
MLA Jiang, Linwen,et al."Synthesis and magnetic properties of nanocrystalline Gd3Fe5O12 and GdFeO3 powders prepared by sol-gel auto-combustion method".MATERIALS RESEARCH BULLETIN 104(2018):92.
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