Study of synthetic diamonds by dynamic nuclear polarization-enhanced C-13 nuclear magnetic resonance spectroscopy
Guo, J; Ye, C; Lu, J; Qiu, J; Yang, B; Zhou, J; Hu, H; Li, L; He, P
刊名APPLIED MAGNETIC RESONANCE
1995
卷号9期号:3页码:379-388
文献子类Article
英文摘要Four I-b-type synthetic diamond crystals were studied by dynamic nuclear polarization (DNP)-enhanced high resolution solid state C-13 nuclear magnetic resonance (NMR) spectroscopy. The home built DNP magic-angle-spinning (MAS) NMR spectrometer operates at a field strength of 1.9 T and the highest DNP enhancement factor of synthetic diamonds came near to 10(3). Comparing with I-b-type natural diamonds, the C-13 NMR linewidths of synthetic diamonds in static spectra are broader. The C-13 spin-lattice relaxation time and DNP polarization time of synthetic diamond are shorter than those of I-b-type natural diamond. From the hyperfine structure of the DNP enhancement curve, four kinds of nitrogen-centred free radicals could be identified in synthetic diamond.
WOS关键词SOLIDS ; NMR
WOS研究方向Physics ; Spectroscopy
语种英语
WOS记录号WOS:A1995TN56000007
内容类型期刊论文
源URL[http://ir.wipm.ac.cn/handle/112942/12073]  
专题武汉物理与数学研究所_2011年以前论文发表(包括2011年)
作者单位CHINESE ACAD SCI,WUHAN INST PHYS,LAB MAGNET RESONANCE & ATOM & MOLEC PHYS,WUHAN 430071,PEOPLES R CHINA
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GB/T 7714
Guo, J,Ye, C,Lu, J,et al. Study of synthetic diamonds by dynamic nuclear polarization-enhanced C-13 nuclear magnetic resonance spectroscopy[J]. APPLIED MAGNETIC RESONANCE,1995,9(3):379-388.
APA Guo, J.,Ye, C.,Lu, J.,Qiu, J.,Yang, B.,...&He, P.(1995).Study of synthetic diamonds by dynamic nuclear polarization-enhanced C-13 nuclear magnetic resonance spectroscopy.APPLIED MAGNETIC RESONANCE,9(3),379-388.
MLA Guo, J,et al."Study of synthetic diamonds by dynamic nuclear polarization-enhanced C-13 nuclear magnetic resonance spectroscopy".APPLIED MAGNETIC RESONANCE 9.3(1995):379-388.
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