LIBS coupled with ICP/OES for the spectral analysis of betel leaves
Khan, M. Z.2; Muhammad, R.2; Sultana, S.3; Rehan, K.1,2,4; Rehan, I.2
刊名APPLIED PHYSICS B-LASERS AND OPTICS
2018-05-01
卷号124期号:5
DOI10.1007/s00340-018-6947-4
文献子类Article
英文摘要Laser-induced breakdown spectroscopy (LIBS) system was optimized and was applied for the elemental analysis and exposure of the heavy metals in betel leaves in air. Pulsed Nd:YAG (1064 nm) in conjunction with a suitable detector (LIBS 2000+, Ocean Optics, Inc) having the optical resolution of 0.06 nm was used to record the emission spectra from 200 to 720 nm. Elements like Al, Ba, Ca, Cr, Cu, P, Fe, K, Mg, Mn, Na, P, S, Sr, and Zn were found to be present in the samples. The abundances of observed elements were calculated through normalized calibration curve method, integrated intensity ratio method, and calibration free-LIBS approach. Quantitative analyses were accomplished under the assumption of local thermodynamic equilibrium (LTE) and optically thin plasma. LIBS findings were validated by comparing its results with the results obtained using a typical analytical technique of inductively coupled plasma-optical emission spectroscopy (ICP/OES). Limit of detection (LOD) of the LIBS system was also estimated for heavy metals.
WOS关键词INDUCED BREAKDOWN SPECTROSCOPY ; TRACE-ELEMENT CONTENTS ; METALS ; SPECTROMETRY ; SAMPLES ; TURKEY ; DIGESTION ; SLURRIES ; QUALITY ; FOODS
WOS研究方向Optics ; Physics
语种英语
WOS记录号WOS:000431906400008
内容类型期刊论文
源URL[http://ir.wipm.ac.cn/handle/112942/12055]  
专题武汉物理与数学研究所_原子分子光物理研究部
作者单位1.Chinese Acad Sci, Wuhan Inst Phys & Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Hubei, Peoples R China
2.Fed Urdu Univ Arts Sci & Technol, Dept Appl Phys, Islamabad 44000, Pakistan
3.Islamia Coll Univ, Dept Chem, Peshawar 25120, Pakistan
4.Univ Chinese Acad Sci, Sch Phys, Beijing 100049, Peoples R China
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Khan, M. Z.,Muhammad, R.,Sultana, S.,et al. LIBS coupled with ICP/OES for the spectral analysis of betel leaves[J]. APPLIED PHYSICS B-LASERS AND OPTICS,2018,124(5).
APA Khan, M. Z.,Muhammad, R.,Sultana, S.,Rehan, K.,&Rehan, I..(2018).LIBS coupled with ICP/OES for the spectral analysis of betel leaves.APPLIED PHYSICS B-LASERS AND OPTICS,124(5).
MLA Khan, M. Z.,et al."LIBS coupled with ICP/OES for the spectral analysis of betel leaves".APPLIED PHYSICS B-LASERS AND OPTICS 124.5(2018).
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