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Ce basic hydroxycarbonate complexe as precursor for mesoporous ceria: Synthesis and characterization
Yang, D. ; Wen, M. F. ; Song, C. L. ; Chen, J. ; Gu, Y. W.
2010-05-10 ; 2010-05-10
会议名称Nanoscience and Technology, Pts 1 and 2 ; China International Conference on Nanoscience and Technology (ChinaNANO 2005) ; Beijing, PEOPLES R CHINA ; Web of Science
关键词mesoporous materials ceria hydroxycarbonate thermal stability OXYGEN STORAGE SURFACE ROUTE Materials Science, Multidisciplinary Physics, Applied Physics, Condensed Matter
中文摘要Herein mesoporous CeO2 with high thermal stability was synthesized via a new hydroxycarbonates based hydrothermal threatment approach in present of hexadecyltrimethylammonium bromide (CTAB). IR and XRD prove the coexistence of hydroxycarbonate cerium and CTAB in precursors. TEM micrographs show that non-ordered pore structure is formed in the product, and average particle size of 20 nm is obtained even after calcined at 1173 K. BET results exhibit that the pore structure is stable when the calcination temperature is below 923 K. However, While calcinated at 1173 K, the average particle size is 20 nm, the BET surface area and pore volume can remain as high as 31.07 m(2)/g and 0.21 cm(3)g(-1).
会议录出版者TRANS TECH PUBLICATIONS LTD ; STAFA-ZURICH ; LAUBLSRUTISTR 24, CH-8717 STAFA-ZURICH, SWITZERLAND
语种英语 ; 英语
内容类型会议论文
源URL[http://hdl.handle.net/123456789/18828]  
专题清华大学
推荐引用方式
GB/T 7714
Yang, D.,Wen, M. F.,Song, C. L.,et al. Ce basic hydroxycarbonate complexe as precursor for mesoporous ceria: Synthesis and characterization[C]. 见:Nanoscience and Technology, Pts 1 and 2, China International Conference on Nanoscience and Technology (ChinaNANO 2005), Beijing, PEOPLES R CHINA, Web of Science.
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