The Non-Destructive Analysis of Some Ancient Jade Artifacts Unearthed from Henan Province by a Variety of Optical Techniques
Wang Kai; Dong Jun-qing; Zhao Hong-xia; Gan Fu-xi; Hu Yong-qing; Fan Wen-quan
刊名光谱学与光谱分析
2015
卷号35期号:9页码:2492
通讯作者gan, fx (reprint author), chinese acad sci, shanghai inst opt & fine mech, ctr sci tech archaeol, shanghai 201800, peoples r china.
英文摘要a total of 14 pieces of ancient jade artifact unearthed from henan province were non-destructively analyzed by means of a portable x-ray fluorescence spectrometer (pxrf), laser raman spectroscopy (portable and mobile) and optical coherence tomography (oct) technology, comprehensively. the raw materials of ancient jade artifacts could be determined accurately through the combination of pxrf and portable raman spectrometer in a short time. with the advantages of small size and easy-operation, these two instruments are suitable to in situ non-destructive analysis of ancient jade artifacts. the results of the pxrf shows that these ancient jade artifacts can be divided into 6 categories such as rich in si al k, rich in ca, rich in si ca, rich in si mg, rich in si, rich in ca p. their main phases have been successfully identified by the portable raman spectrometer. in the lab, the mobile confocal laser raman spectrometer, which help us find the raman vibration peak of [oh] in the tremolite jade, is used to make up the disadvantages of the portable raman spectrometer such as lower spectral resolution, lower accuracy and narrower measuring range. we can use the oct to analyze the transparency, fiber fineness and inclusion etc. of the jade artifacts. the confocal laser raman spectroscopy combined with oct is used to analyze 2 containing inclusion of tremolite jade samples. oct image can visually display the distribution characteristics of the inclusion in these 2 samples. confocal laser raman spectroscopy can accurately locate the sample surface of inclusion, then we can observe the micro morphology and analyze its phase. the results show that the black inclusion is graphite. this work is very significant to study the geographical origin of jade. through the study we find, the use of ocrf, laser raman spectroscopy (portable and mobile) and oct can be achieved on the identification and analysis of cultural relic's phase composition and texture feature and meet the basic requirements of field archaeological work analysis.
收录类别SCI
语种中文
内容类型期刊论文
版本出版稿
源URL[http://ir.siom.ac.cn/handle/181231/13922]  
专题上海光学精密机械研究所_高密度光存储技术实验室
作者单位1.[Wang Kai
2.Dong Jun-qing
3.Zhao Hong-xia
4.Gan Fu-xi] Chinese Acad Sci, Shanghai Inst Opt & Fine Mech, Ctr Sci Tech Archaeol, Shanghai 201800, Peoples R China
5.[Gan Fu-xi] Fudan Univ, Dept Opt Sci & Engn, Shanghai 200433, Peoples R China
6.[Hu Yong-qing
7.Fan Wen-quan] Inst Cultural Rel Henan Prov, Zhengzhou 450000, Peoples R China
推荐引用方式
GB/T 7714
Wang Kai,Dong Jun-qing,Zhao Hong-xia,et al. The Non-Destructive Analysis of Some Ancient Jade Artifacts Unearthed from Henan Province by a Variety of Optical Techniques[J]. 光谱学与光谱分析,2015,35(9):2492.
APA Wang Kai,Dong Jun-qing,Zhao Hong-xia,Gan Fu-xi,Hu Yong-qing,&Fan Wen-quan.(2015).The Non-Destructive Analysis of Some Ancient Jade Artifacts Unearthed from Henan Province by a Variety of Optical Techniques.光谱学与光谱分析,35(9),2492.
MLA Wang Kai,et al."The Non-Destructive Analysis of Some Ancient Jade Artifacts Unearthed from Henan Province by a Variety of Optical Techniques".光谱学与光谱分析 35.9(2015):2492.
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