Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction | |
Chen F(陈飞); 徐殿斗;Chen, F; Xu, DD; Tang, XP; Cao, J; Liu, YT; Deng, J | |
刊名 | SPECTROSCOPY AND SPECTRAL ANALYSIS |
2012 | |
卷号 | 32期号:1页码:239-243 |
关键词 | ICP-OES Heavy metals Textiles Microwave-assisted extraction |
英文摘要 | Textiles are easily contaminated by heavy metals in the course of processing. In order to monitor the quality of textiles, a new method was developed for simultaneous determination of arsenic, antimony, lead, cadmium, chromium, cobalt, copper, nickel and mercury in textiles by inductively coupled plasma optical emission spectrometry (ICP-OES) after microwave-assisted dilute nitric acid extraction. After optimizing extraction conditions, we ultimately selected 5% nitric acid as extractant and 5 mm as extraction time with the extraction temperature of 120 degrees C and instrument power of 400W in the microwave-assisted extraction procedure. Nine hazardous elements were detected sequentially by ICP-OES. The results showed that the detection limits were 0.3 similar to 15 mu g . L(-1) and the recoveries 73.6%similar to 105% with the RSDs (n=3) of 0.1%similar to 3%. The proposed method was successfully used to determine nine elements in cotton, wool, terylene and acrylic. |
学科主题 | Spectroscopy |
收录类别 | SCI |
WOS记录号 | WOS:000298900300054 |
公开日期 | 2016-05-03 |
内容类型 | 期刊论文 |
源URL | [http://ir.ihep.ac.cn/handle/311005/223903] |
专题 | 高能物理研究所_核技术应用研究中心 高能物理研究所_多学科研究中心 |
推荐引用方式 GB/T 7714 | Chen F,徐殿斗;Chen, F,Xu, DD,et al. Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS,2012,32(1):239-243. |
APA | 陈飞.,徐殿斗;Chen, F.,Xu, DD.,Tang, XP.,Cao, J.,...&Deng, J.(2012).Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction.SPECTROSCOPY AND SPECTRAL ANALYSIS,32(1),239-243. |
MLA | 陈飞,et al."Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction".SPECTROSCOPY AND SPECTRAL ANALYSIS 32.1(2012):239-243. |
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