Development of a more specific and accurate multiple reaction monitoring method based on GC-EI/MS/MS for simultaneously monitoring and determining 34 kinds of pesticides in Qianjinzhidai pills

CORC > 兰州化学物理研究所 > 中国科学院兰州化学物理研究所 > 非现建制

	Development of a more specific and accurate multiple reaction monitoring method based on GC-EI/MS/MS for simultaneously monitoring and determining 34 kinds of pesticides in Qianjinzhidai pills
	Jiang, Yunbin 1; Zhong, Mei 2,3; Gou, Yan 4; Peng, Wei 1; Zhou, Juan 4; Wu, Pie 4; Ma, Yuying 1
刊名	Journal of Chromatography B
	2015
卷号	983 页码:47-54
关键词	GC-EI/MS/MS Pesticide residues Ion transitions Monitoring Content determination Qianjinzhidai pills
ISSN号	1570-0232
通讯作者	Ma, Yuying
英文摘要	A rapid and accurate multi-residue method was developed for simultaneously monitoring and determining 34 kinds of pesticides by GC–EI/MS/MS, successfully applied in Qianjinzhidai pills. Precision, repeatability, stability, limit of detection (LOD), limit of quantification (LOQ), linearity range and accuracy tests were used to validate this method. The results, precision (RSD < 2%, n = 6), repeatability (RSD < 2%, n = 6) and stability (RSD < 2%, n = 6), LOD (lower than 0.02 mg/kg), LOQ (lower than 0.067 mg/kg), linearity range (0.016–39.270 μg/mL), recoveries (90–110%, RSD < 15%, n = 6), indicated that the method was feasible. This paper provided an optimization method about ion transitions which can improve the specificity of mass spectrum monitoring and the accuracy of content determination. This method can be also used to monitor and determine pesticide residues of other traditional Chinese medicine, but it was worth noting that the ion transitions should been again optimized according to the sample matrix.
收录类别	SCI
语种	英语
WOS记录号	WOS:000349506200007
内容类型	期刊论文
源URL	[http://210.77.64.217/handle/362003/19301]
专题	兰州化学物理研究所_非现建制
作者单位	1.Chengdu Univ Tradit Chinese Med, Chengdu 611137, Peoples R China 2.Chinese Acad Sci, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China 3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China 4.Sichuan Prov Inst Food & Drug Control, Chengdu 610079, Peoples R China
推荐引用方式 GB/T 7714	Jiang, Yunbin,Zhong, Mei,Gou, Yan,et al. Development of a more specific and accurate multiple reaction monitoring method based on GC-EI/MS/MS for simultaneously monitoring and determining 34 kinds of pesticides in Qianjinzhidai pills[J]. Journal of Chromatography B,2015,983:47-54.
APA	Jiang, Yunbin.,Zhong, Mei.,Gou, Yan.,Peng, Wei.,Zhou, Juan.,...&Ma, Yuying.(2015).Development of a more specific and accurate multiple reaction monitoring method based on GC-EI/MS/MS for simultaneously monitoring and determining 34 kinds of pesticides in Qianjinzhidai pills.Journal of Chromatography B,983,47-54.
MLA	Jiang, Yunbin,et al."Development of a more specific and accurate multiple reaction monitoring method based on GC-EI/MS/MS for simultaneously monitoring and determining 34 kinds of pesticides in Qianjinzhidai pills".Journal of Chromatography B 983(2015):47-54.